(E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.1^3,8]undec-4-yl)-3-phenyl-propenone

Base Information

• Chemical Name: (E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.1^3,8]undec-4-yl)-3-phenyl-propenone
• CAS No.: 112237-97-5
• Molecular Formula: C₂₀H₂₃NO
• Molecular Weight: 293.409

Synonyms:(E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.1^3,8]undec-4-yl)-3-phenyl-propenone

Chemical Property of (E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.1^3,8]undec-4-yl)-3-phenyl-propenone

Chemical Property:

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Technology Process of (E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.1^3,8]undec-4-yl)-3-phenyl-propenone

There total 1 articles about (E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.1^3,8]undec-4-yl)-3-phenyl-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

cinnamoyl chloride (102-92-1,17082-09-6) + 5-methyl-4-azatricyclo<4.3.1.13,8>undec-4-ene (65218-97-5) → (E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.13,8]undec-4-yl)-3-phenyl-propenone (112237-97-5)

Guidance literature:

With triethylamine; In diethyl ether; 1.) ice cooling, 2.) room temp., 3 h;

Reference yield: 61.0%

(E)-1-((1S,3R,6S,8R)-5-Methylene-4-aza-tricyclo[4.3.1.13,8]undec-4-yl)-3-phenyl-propenone (112237-97-5) → (E)-1-(1R,3R,6S,8S)-4-Aza-tricyclo[4.3.1.13,8]undec-(5Z)-ylidene-4-phenyl-but-3-en-2-one (112238-76-3)

Guidance literature:

In diethyl ether; for 1.5h; Irradiation;

upstream raw materials:

cinnamoyl chloride

5-methyl-4-azatricyclo<4.3.1.1^3,8>undec-4-ene

Downstream raw materials:

(E)-1-(1R,3R,6S,8S)-4-Aza-tricyclo[4.3.1.1^3,8]undec-(5Z)-ylidene-4-phenyl-but-3-en-2-one

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