(tripod)Co(CCC(CH₃)3)2

Base Information

Chemical Name:(tripod)Co(CCC(CH₃)3)2
CAS No.:307556-06-5
Molecular Formula:C₅₃H₅₇CoP₃
Molecular Weight:845.95
Hs Code.:

Synonyms:(tripod)Co(CCC(CH₃)3)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (tripod)Co(CCC(CH₃)3)2

Chemical Property:

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Technology Process of (tripod)Co(CCC(CH₃)3)2

There total 1 articles about (tripod)Co(CCC(CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917-92-0
3,3-Dimethylbut-1-yne

: 197300-99-5,27427-44-7
(tripod)CoCl₂

: 307556-06-5
(tripod)Co(CCC(CH₃)3)2

Guidance literature:: With n-BuLi; In tetrahydrofuran; diethyl ether; hexane; byproducts: LiCl; under Ar, 2 equiv. of alkyne in Et2O was deprotonated with n-BuLi (2.5 Min hexane) at -80 °C, after 5 min mixt. was allowed to warm to r oom temp., Co-salt was added in THF at -80 °C, after 10 min soln.was allowed to stand to room temp.; solvent was evapd. in vac., residue was dissolved in toluene, LiCl was filtered off, solvent was evapd., elem. anal.;
DOI:10.1002/1099-0682(200009)2000:9<1953::aid-ejic1953>3.0.co;2-1

Reference yield:

: 307556-06-5
(tripod)Co(CCC(CH₃)3)2

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: [(tripod)Co(CCBu-t)2Ni(CO)]

Guidance literature:: In toluene; byproducts: CO; 3-fold excess of Ni(CO)4 was used, stirring for 2 h, under Ar; solvent was removed in vac., recrystn. from CH2Cl2, solvent was evapd., elem. anal.;
DOI:10.1002/1099-0682(200009)2000:9<1953::aid-ejic1953>3.0.co;2-1