Nb[C₆H₃(CH₃)3]2(CO)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(CO)(C₆H₃(CH₃)3)2][B(C₆H₄F)4]

Base Information

• Chemical Name: Nb[C₆H₃(CH₃)3]2(CO)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(CO)(C₆H₃(CH₃)3)2][B(C₆H₄F)4]
• CAS No.: 156301-43-8
• Molecular Formula: C₁₉H₂₄NbO*C₂₄H₁₆BF₄
• Molecular Weight: 752.501
• Mol file: 156301-43-8.mol

Synonyms:Nb[C₆H₃(CH₃)3]2(CO)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(CO)(C₆H₃(CH₃)3)2][B(C₆H₄F)4]

Chemical Property of Nb[C₆H₃(CH₃)3]2(CO)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(CO)(C₆H₃(CH₃)3)2][B(C₆H₄F)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Nb[C₆H₃(CH₃)3]2(CO)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(CO)(C₆H₃(CH₃)3)2][B(C₆H₄F)4]

There total 2 articles about Nb[C₆H₃(CH₃)3]2(CO)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(CO)(C₆H₃(CH₃)3)2][B(C₆H₄F)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nb[C6H3(CH3)3]2(C6H5CCC6H5)(1+)*B(C6H4F)4(1-)*C7H8=[Nb(C6H3(CH3)3)2(C6H5CCC6H5)][B(C6H4F)4]*C7H8 → Nb[C6H3(CH3)3]2(CO)(1+)*B(C6H4F)4(1-)=[Nb(CO)(C6H3(CH3)3)2][B(C6H4F)4] (156301-43-8)

Guidance literature:

With CO; In not given;

Reference yield:

Nb[C6H3(CH3)3]2(1+)*B(C6H4F)4(1-)=[Nb(C6H3(CH3)3)2][B(C6H4F)4] (156301-38-1) → Nb[C6H3(CH3)3]2(CO)(1+)*B(C6H4F)4(1-)=[Nb(CO)(C6H3(CH3)3)2][B(C6H4F)4] (156301-43-8)

Guidance literature:

With CO; In toluene; under Ar; absorption of CO by Nb-complex/toluene at 22.4°C;

Reference yield: 94.0%

dimethylacetylene (503-17-3) + Nb[C6H3(CH3)3]2(CO)(1+)*B(C6H4F)4(1-)=[Nb(CO)(C6H3(CH3)3)2][B(C6H4F)4] (156301-43-8) → Nb[C6H3(CH3)3]2(CH3CCCH3)(1+)*B(C6H4F)4(1-)=[Nb(C6H3(CH3)3)2(CH3CCCH3)][B(C6H4F)4] (156301-41-6)

Guidance literature:

In toluene; under Ar; suspn. Nb-complex/toluene treated with but-2-yne, mixt. stirred; filtered, dried (vac., room temp.), elem. anal.;

upstream raw materials:

Nb[C₆H₃(CH₃)3]2⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(C₆H₃(CH₃)3)2][B(C₆H₄F)4]

Downstream raw materials:

Nb[C₆H₃(CH₃)3]2(CH₃CCCH₃)⁽¹⁺⁾*B(C₆H₄F)4^(1-)=[Nb(C₆H₃(CH₃)3)2(CH₃CCCH₃)][B(C₆H₄F)4]