methyl -o-toluate

Base Information

Chemical Name:methyl -o-toluate
CAS No.:136391-75-8
Molecular Formula:C₉H₁₀O₂
Molecular Weight:151.166
Hs Code.:

Synonyms:methyl -o-toluate

Suppliers and Price of methyl -o-toluate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl -o-toluate

Chemical Property:

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Technology Process of methyl -o-toluate

There total 1 articles about methyl -o-toluate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 70838-82-3
-o-toluic acid

: 136391-75-8
methyl -o-toluate

Guidance literature:

Reference yield: 90.0%

: 136391-75-8
methyl -o-toluate

: 339222-04-7
o-methyl<α-13C>benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;
DOI:10.1021/ja0039482

Reference yield:

: 136391-75-8
methyl -o-toluate

: 339222-05-8
[1-13C] 1-(2'-methylphenyl)-2,2,4-trimethylpentan-3-on-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / LiAlH₄ / tetrahydrofuran / Heating

2.1: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

3.1: EtMgBr / benzene / 0.5 h / 15 °C

3.2: 80 percent / benzene / 1 h / -5 °C

With lithium aluminium tetrahydride; ethylmagnesium bromide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja0039482