(R)-methyl 2-propionyloxy-2-phenylethanoate

Base Information

Chemical Name:(R)-methyl 2-propionyloxy-2-phenylethanoate
CAS No.:133797-12-3
Molecular Formula:C₁₂H₁₄O₄
Molecular Weight:222.241
Hs Code.:

Synonyms:(R)-methyl 2-propionyloxy-2-phenylethanoate

Suppliers and Price of (R)-methyl 2-propionyloxy-2-phenylethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-methyl 2-propionyloxy-2-phenylethanoate

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Technology Process of (R)-methyl 2-propionyloxy-2-phenylethanoate

There total 5 articles about (R)-methyl 2-propionyloxy-2-phenylethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 22979-35-7
Methyl phenyldiazoacetate

: 802294-64-0,79-09-4
propionic acid

: 85805-92-1,133797-12-3
2-methoxy-2-oxo-1-phenylethyl propionate

Guidance literature:: With tropylium tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c04069

Reference yield:

: 20698-91-3
(R)-methyl mandelate

: 802294-64-0,79-09-4
propionic acid

: 133797-12-3
(R)-methyl 2-propionyloxy-2-phenylethanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 3h;
DOI:10.1021/ja00012a032

Reference yield:

: 1359987-72-6
C₂₂H₃₈O₂Sn

: 85805-92-1,133797-12-3
2-methoxy-2-oxo-1-phenylethyl propionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: cesium fluoride / N,N-dimethyl-formamide / 6 h / 60 °C / 750.08 Torr

1.2: 0 °C / pH 2 / Inert atmosphere

2.1: methanol; diethyl ether / 1 h / Inert atmosphere

With cesium fluoride; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo202597p