2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

Base Information

Chemical Name:2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide
CAS No.:756481-41-1
Molecular Formula:C₂₃H₃₆N₄O
Molecular Weight:384.565
Hs Code.:

Synonyms:2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

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Chemical Property of 2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

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Technology Process of 2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

There total 8 articles about 2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 532983-09-8
8-ethyl-7-(4-heptyl)-1-methyl-3-(2,4,6-trimethylphenyl)-3,7-dihydro-1H-purine-2,6-dione

: 756481-41-1
2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/jm049787k

Reference yield:

: 67764-22-1
4-heptylmethane sulphonate

: 756481-41-1
2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 90 °C

2: 64 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm049787k

Reference yield:

: 2958-62-5
mesityl isocyanate

: 756481-41-1
2-ethyl-1-(4-heptyl)-N-methyl-4-[(2,4,6-trimethylphenyl)amino]-1H-imidazole-5-carboxamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethanol; tetrahydrofuran / 65 °C

2.1: acetic anhydride / 85 °C

2.2: 20 percent NaOH / 70 °C

3.1: aq. NaNO₂; acetic acid / 50 - 75 °C

4.1: aq. NH₄OH; Na₂S₂O₄ / 50 °C

5.1: ethanol / Heating

6.1: K₂CO₃ / dimethylformamide / 90 °C

7.1: 64 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 20 °C

With ammonium hydroxide; lithium aluminium tetrahydride; sodium dithionite; acetic anhydride; potassium carbonate; acetic acid; sodium nitrite; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm049787k