C₃₈H₆₁NO₃S₂Si

Base Information

Chemical Name:C₃₈H₆₁NO₃S₂Si
CAS No.:1351657-17-4
Molecular Formula:C₃₈H₆₁NO₃S₂Si
Molecular Weight:672.125
Hs Code.:

C<sub>38</sub>H<sub>61</sub>NO<sub>3</sub>S<sub>2</sub>Si

Synonyms:C₃₈H₆₁NO₃S₂Si

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Chemical Property of C₃₈H₆₁NO₃S₂Si

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Technology Process of C₃₈H₆₁NO₃S₂Si

There total 28 articles about C₃₈H₆₁NO₃S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80657-88-1
(2R,4R)-2-Methyl-4-((4S,5R)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-pentan-1-ol

: 1351657-17-4
C₃₈H₆₁NO₃S₂Si

Guidance literature:: Multi-step reaction with 23 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride / tetrahydrofuran

4: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

5: pyridine; tributylphosphine

6: dichloromethane

7: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

8: sodium periodate / methanol; water

9: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

10: sodium hydride / tetrahydrofuran

11: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

12: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

13: lithium diisopropyl amide / tetrahydrofuran

14: lithium aluminium tetrahydride / tetrahydrofuran

15: 1H-imidazole / dichloromethane

16: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

17: tetrabutyl ammonium fluoride / tetrahydrofuran

18: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

19: hydrogenchloride / methanol

20: 2,6-dimethylpyridine / dichloromethane

21: pyridine; pyridine hydrogenfluoride / tetrahydrofuran

22: Dess-Martin periodane / dichloromethane

23: tetrahydrofuran / 0 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; pyridine hydrogenfluoride; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 1: Swern oxidation / 2: Horner-Emmons olefination / 4: Katsuki-Sharpless epoxidation / 9: Pummerer rearrangement / 10: Horner-Emmons olefination / 22: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: 1351656-96-6
C₁₄H₂₆O₄

: 1351657-17-4
C₃₈H₆₁NO₃S₂Si

Guidance literature:: Multi-step reaction with 24 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

3: sodium hydride / tetrahydrofuran

4: diisobutylaluminium hydride / tetrahydrofuran

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

6: pyridine; tributylphosphine

7: dichloromethane

8: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

9: sodium periodate / methanol; water

10: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

11: sodium hydride / tetrahydrofuran

12: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

13: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

14: lithium diisopropyl amide / tetrahydrofuran

15: lithium aluminium tetrahydride / tetrahydrofuran

16: 1H-imidazole / dichloromethane

17: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

18: tetrabutyl ammonium fluoride / tetrahydrofuran

19: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

20: hydrogenchloride / methanol

21: 2,6-dimethylpyridine / dichloromethane

22: pyridine; pyridine hydrogenfluoride / tetrahydrofuran

23: Dess-Martin periodane / dichloromethane

24: tetrahydrofuran / 0 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; pyridine hydrogenfluoride; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 2: Swern oxidation / 3: Horner-Emmons olefination / 5: Katsuki-Sharpless epoxidation / 10: Pummerer rearrangement / 11: Horner-Emmons olefination / 23: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: C₁₇H₃₀O₄

: 1351657-17-4
C₃₈H₆₁NO₃S₂Si

Guidance literature:: Multi-step reaction with 21 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

3: pyridine; tributylphosphine

4: dichloromethane

5: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

6: sodium periodate / methanol; water

7: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

8: sodium hydride / tetrahydrofuran

9: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

10: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

11: lithium diisopropyl amide / tetrahydrofuran

12: lithium aluminium tetrahydride / tetrahydrofuran

13: 1H-imidazole / dichloromethane

14: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

15: tetrabutyl ammonium fluoride / tetrahydrofuran

16: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

17: hydrogenchloride / methanol

18: 2,6-dimethylpyridine / dichloromethane

19: pyridine; pyridine hydrogenfluoride / tetrahydrofuran

20: Dess-Martin periodane / dichloromethane

21: tetrahydrofuran / 0 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; pyridine hydrogenfluoride; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 2: Katsuki-Sharpless epoxidation / 7: Pummerer rearrangement / 8: Horner-Emmons olefination / 20: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.10.073