N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

Base Information

Chemical Name:N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide
CAS No.:176198-89-3
Molecular Formula:C₁₄H₁₉NO₅
Molecular Weight:281.309
Hs Code.:

Synonyms:N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

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Technology Process of N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

There total 5 articles about N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 175981-99-4
N-((2S,3S,4R,5S,6R)-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-phenyltetrahydro-2H-pyran-3-yl)acetamide

: 176198-89-3
N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1039/CC9960000347

Reference yield:

: 591-51-5
phenyllithium

: 176198-89-3
N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85.4 percent / toluene / 1 h / -78 °C

2: 91 percent / Et₃SiH, BF₃*Et₂O / acetonitrile / 0.25 h / -40 °C

3: 75 percent / H₂ / Raney Ni

4: 89 percent / H₂ / Pd/C / tetrahydrofuran

With triethylsilane; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; nickel; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1039/CC9960000347

Reference yield:

: 160701-84-8
(3R,4R,5R,6R)-3-azido-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 176198-89-3
N-((2S,3R,4R,5R,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenyl-tetrahydro-pyran-3-yl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85.4 percent / toluene / 1 h / -78 °C

2: 91 percent / Et₃SiH, BF₃*Et₂O / acetonitrile / 0.25 h / -40 °C

3: 75 percent / H₂ / Raney Ni

4: 89 percent / H₂ / Pd/C / tetrahydrofuran

With triethylsilane; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; nickel; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1039/CC9960000347