Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate

Base Information

• Chemical Name: Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate
• CAS No.: 91715-39-8
• Molecular Formula: C₁₅H₉BrCl₂NO₃*Na
• Molecular Weight: 425.041

Synonyms:Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate

Chemical Property of Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate

Chemical Property:

Purity/Quality:

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Technology Process of Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate

There total 7 articles about Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

7-(4-Bromo-2-chloro-benzoyl)-5-chloro-1,3-dihydro-indol-2-one (91714-36-2) → Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate (91715-39-8)

Guidance literature:

With sodium hydroxide; for 18h; Heating;

DOI:10.1021/jm00377a001

Reference yield:

1-indoline (496-15-1) → Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate (91715-39-8)

Guidance literature:

Multi-step reaction with 6 steps

1: 1.) BCl₃, AlCl₃, 2.) aq. HCl / 1.) toluene, reflux, 20 h, 2.) toluene, reflux, 2.5 h

2: 68 percent / N-chlorosuccinimide / CH₂Cl₂ / Ambient temperature

3: 99 percent / MnO₂ / CH₂Cl₂ / Heating

4: 99 percent / N-bromosuccinimide / CH₂Cl₂ / Ambient temperature

5: 33 percent / 86percent aq. phosphoric acid / 2-methoxy-ethanol / 18 h / Heating

6: 69 percent / 3N aq. NaOH / 18 h / Heating

With hydrogenchloride; manganese(IV) oxide; sodium hydroxide; N-chloro-succinimide; N-Bromosuccinimide; aluminium trichloride; phosphoric acid; boron trichloride; In dichloromethane; 2-methoxy-ethanol;

DOI:10.1021/jm00377a001

Reference yield:

4-bromo-2-chlorobenzonitrile (154607-01-9) → Sodium; [2-amino-3-(4-bromo-2-chloro-benzoyl)-5-chloro-phenyl]-acetate (91715-39-8)

Guidance literature:

Multi-step reaction with 6 steps

1: 1.) BCl₃, AlCl₃, 2.) aq. HCl / 1.) toluene, reflux, 20 h, 2.) toluene, reflux, 2.5 h

2: 68 percent / N-chlorosuccinimide / CH₂Cl₂ / Ambient temperature

3: 99 percent / MnO₂ / CH₂Cl₂ / Heating

4: 99 percent / N-bromosuccinimide / CH₂Cl₂ / Ambient temperature

5: 33 percent / 86percent aq. phosphoric acid / 2-methoxy-ethanol / 18 h / Heating

6: 69 percent / 3N aq. NaOH / 18 h / Heating

With hydrogenchloride; manganese(IV) oxide; sodium hydroxide; N-chloro-succinimide; N-Bromosuccinimide; aluminium trichloride; phosphoric acid; boron trichloride; In dichloromethane; 2-methoxy-ethanol;

DOI:10.1021/jm00377a001

upstream raw materials:

7-(4-Bromo-2-chloro-benzoyl)-5-chloro-1,3-dihydro-indol-2-one

1-indoline

4-bromo-2-chlorobenzonitrile

(4-Bromo-2-chloro-phenyl)-(2,3-dihydro-1H-indol-7-yl)-methanone

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