2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid

Base Information

• Chemical Name: 2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid
• CAS No.: 1044550-60-8
• Molecular Formula: C₂₇H₂₀N₂O₅
• Molecular Weight: 452.466

Synonyms:2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid

Chemical Property of 2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid

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Technology Process of 2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid

There total 1 articles about 2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3-(2-formylphenyl)-4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-1H-pyrrole-2,5-dione (1044550-55-1) → 2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid (1044550-60-8)

Guidance literature:

With sodium chlorite; aminosulfonic acid; water; In 1,4-dioxane; at 2 ℃; for 0.0166667h;

DOI:10.1039/b801121d

Reference yield: 95.0%

2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid (1044550-60-8) → 2-[4-(5-benzyloxy-1H-indol-3-yl)-2,5-dioxo-2,5-dihydrofuran-3-yl]benzoic acid (1044550-62-0)

Guidance literature:

2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid; With potassium hydroxide; water; In acetone; at 20 ℃; for 24h;

With hydrogenchloride; water; at 20 ℃; for 24h; pH=1;

DOI:10.1039/b801121d

Reference yield: 83.0%

2-[4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid (1044550-60-8) → 2-[4-(5-hydroxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid (1044550-64-2)

Guidance literature:

With boron tribromide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/b801121d

upstream raw materials:

3-(2-formylphenyl)-4-(5-benzyloxy-1H-indol-3-yl)-1-methyl-1H-pyrrole-2,5-dione

Downstream raw materials:

2-[4-(5-benzyloxy-1H-indol-3-yl)-2,5-dioxo-2,5-dihydrofuran-3-yl]benzoic acid

2-[4-(5-hydroxy-1H-indol-3-yl)-1-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl]benzoic acid

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