(E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene

Base Information

• Chemical Name: (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene
• CAS No.: 755022-08-3
• Molecular Formula: C₃₆H₄₀N₄O₆S₃
• Molecular Weight: 720.935

Synonyms:(E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene

Chemical Property of (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene

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Technology Process of (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene

There total 2 articles about (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sulfanilamide (63-74-1) → (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene (755022-08-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 75 percent / acetic acid / Heating

2: 12 percent / K₂CO₃ / acetonitrile / 23 h / Heating

3: 88 percent / K₂CO₃ / acetonitrile / 24 h / Heating

With potassium carbonate; In acetic acid; acetonitrile;

DOI:10.1002/ejic.200300724

Reference yield:

(4-pyrrol-1-ylphenyl)sulfonamide (5438-30-2) → (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene (755022-08-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 12 percent / K₂CO₃ / acetonitrile / 23 h / Heating

2: 88 percent / K₂CO₃ / acetonitrile / 24 h / Heating

With potassium carbonate; In acetonitrile;

DOI:10.1002/ejic.200300724

Reference yield: 78.0%

bis(dibenzylideneacetone)-palladium(0) (32005-36-0) + (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene (755022-08-3) → (E,E,E)-1,6-bis[(4-methylphenyl)sulfonyl]-11-[(4-pyrrol-1-ylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-trienepalladium(0) dichloromethane

Guidance literature:

In tetrahydrofuran; 1.2 equiv. of Pd compd., refluxed for 1 h; elem. anal.;

DOI:10.1002/ejic.200300724

upstream raw materials:

(4-pyrrol-1-ylphenyl)sulfonamide

sulfanilamide

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