Technology Process of C20H20OSi
There total 3 articles about C20H20OSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C26H28O4SSi;
With
diethyl chlorophosphate;
In
tetrahydrofuran;
at 20 ℃;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at 30 ℃;
Further stages.;
DOI:10.1055/s-2007-986641
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hexamethyldisilazide / tetrahydrofuran / -78 °C
1.2: tetrahydrofuran
2.1: ClP(O)(OEt)2 / tetrahydrofuran / 20 °C
2.2: lithium hexamethyldisilazide / tetrahydrofuran / 30 °C
With
diethyl chlorophosphate; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1055/s-2007-986641
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hexamethyldisilazide / tetrahydrofuran / -78 °C
1.2: tetrahydrofuran
2.1: ClP(O)(OEt)2 / tetrahydrofuran / 20 °C
2.2: lithium hexamethyldisilazide / tetrahydrofuran / 30 °C
With
diethyl chlorophosphate; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1055/s-2007-986641