1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene

Base Information

• Chemical Name: 1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene
• CAS No.: 1028333-65-4
• Molecular Formula: C₂₁H₂₀Cl₂
• Molecular Weight: 343.296

Synonyms:1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene

Chemical Property of 1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene

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Technology Process of 1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene

There total 1 articles about 1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-Dimethyl-2-butene (563-79-1) + C15H10Br2Cl2 → 1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene (1028333-65-4)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1021/jo800390c

Reference yield: 53.0%

1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene (1028333-65-4) + acetonitrile (75-05-8,26809-02-9) → 4-(2-(2-chlorophenyl)-2-(4-chlorophenyl)vinylidene)-2,2,3,3,5-pentamethyl-3,4-dihydro-2H-pyrrole (1028333-74-5) + N-(6-(2-chlorophenyl)-6-(4-chlorophenyl)-2,3,3-trimethylhex-4-yn-2-yl)acetamide (1028333-75-6)

Guidance literature:

With trifluorormethanesulfonic acid; for 0.166667h; Heating;

DOI:10.1021/jo800390c

Reference yield: 34.0%

1-chloro-4-(1-(2-chlorophenyl)-2-(2,2,3,3-tetramethylcyclopropylidene)vinyl)benzene (1028333-65-4) + ethyl 5,5-diphenylpenta-2,3,4-trienoate (1119249-36-3) → (E)-ethyl 2-(3-((2-chlorophenyl)(4-chlorophenyl)methylene)-1,1-dimethyl-8-phenyl-2-(propan-2-ylidene)-1,2,3,3a-tetrahydrocyclopenta[a]inden-3a-yl)acetate (1160169-92-5)

Guidance literature:

With bis(trifluoromethanesulfonyl)amide; In dichloromethane; at 25 ℃; for 12h;

DOI:10.1039/b903965a

upstream raw materials:

2,3-Dimethyl-2-butene

Downstream raw materials:

4-(2-(2-chlorophenyl)-2-(4-chlorophenyl)vinylidene)-2,2,3,3,5-pentamethyl-3,4-dihydro-2H-pyrrole

N-(6-(2-chlorophenyl)-6-(4-chlorophenyl)-2,3,3-trimethylhex-4-yn-2-yl)acetamide

C₄₂H₃₄Cl₂

(E)-ethyl 2-(3-((2-chlorophenyl)(4-chlorophenyl)methylene)-1,1-dimethyl-8-phenyl-2-(propan-2-ylidene)-1,2,3,3a-tetrahydrocyclopenta[a]inden-3a-yl)acetate

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