Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

Base Information

Chemical Name:Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate
CAS No.:97690-87-4
Molecular Formula:C₃₁H₃₄O₄
Molecular Weight:470.609
Hs Code.:

Synonyms:Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

Chemical Property:

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Technology Process of Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

There total 10 articles about Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97805-13-5
(2S,3S,4S)-3,5-isopropylidenedioxy-2,4-dimethyl-1-pentanol

: 97690-87-4
Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

Guidance literature:: Multi-step reaction with 4 steps

1: Swern oxidation

3: p-TsOH / methanol

4: acetonitrile / 1 h / 20 °C

With toluene-4-sulfonic acid; In methanol; acetonitrile;
DOI:10.1021/ja00304a054

Reference yield:

: 97805-14-6
(2R,3R,4S)-3,5-Isopropylidenedioxy-2,4-dimethylpentanal

: 97690-87-4
Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

Guidance literature:: Multi-step reaction with 3 steps

2: p-TsOH / methanol

3: acetonitrile / 1 h / 20 °C

With toluene-4-sulfonic acid; In methanol; acetonitrile;
DOI:10.1021/ja00304a054

Reference yield:

: 72967-11-4
(3-methoxycarbonyl-2-propenyl)triphenylphosphonium bromide

: 97690-87-4
Methyl (2E,4E,6S,7S,8S)-7-hydroxy-6,8-dimethyl-9-triphenylmethoxy-2,4-nonadienoate

Guidance literature:: Multi-step reaction with 3 steps

2: p-TsOH / methanol

3: acetonitrile / 1 h / 20 °C

With toluene-4-sulfonic acid; In methanol; acetonitrile;
DOI:10.1021/ja00304a054