Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester

Base Information

Chemical Name:Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester
CAS No.:870556-91-5
Molecular Formula:C₄₈H₈₀O₅
Molecular Weight:737.16
Hs Code.:

Synonyms:Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester

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Chemical Property of Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester

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Technology Process of Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester

There total 2 articles about Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 870556-89-1
2-Methyl-6-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-benzene-1,4-diol

: 57-11-4
stearic acid

: 870556-91-5
Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In chloroform; at 20 ℃; for 4h;
DOI:10.1248/cpb.53.1159

Reference yield:

: 2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-benzene-1,4-diol

: 870556-91-5
Octadecanoic acid 4-hydroxy-3-methyl-5-[(2E,6E,10E)-3,7,11-trimethyl-13-((R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl)-trideca-2,6,10-trienyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / p-tolenesulfonic acid monohydrate / methanol / 0.5 h / 20 °C

2: 92 percent / N,N'-dicyclohexylcarbodiimide; DMAP / CHCl₃ / 4 h / 20 °C

With dmap; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In methanol; chloroform;
DOI:10.1248/cpb.53.1159