1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

Base Information

Chemical Name:1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane
CAS No.:1642593-65-4
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

Synonyms:1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

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Chemical Property of 1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

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Technology Process of 1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

There total 4 articles about 1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1642593-52-9
2,4-dimethoxy-1-(6-methylhepta-1,5-dien-2-yl)benzene

: 1642593-65-4
1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

Guidance literature:: With oxygen; 2,4,6-tri-(p-methoxyphenyl) pyrylium tetrafluoroborate; In 1,2-dichloro-ethane; at -10 ℃; for 3h; under 760.051 Torr; Inert atmosphere; UV-irradiation;
DOI:10.3762/bjoc.10.128

Reference yield:

: 206051-18-5
N-methoxy-N-methyl-2,4-dimethoxybenzamide

: 1642593-65-4
1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 0 °C / Inert atmosphere

1.2: 18 h / 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.2: 16 h / 0 - 20 °C / Inert atmosphere

3.1: 2,4,6-tri-(p-methoxyphenyl) pyrylium tetrafluoroborate; oxygen / 1,2-dichloro-ethane / 3 h / -10 °C / 760.05 Torr / Inert atmosphere; UV-irradiation

With potassium tert-butylate; oxygen; 2,4,6-tri-(p-methoxyphenyl) pyrylium tetrafluoroborate; magnesium; ethylene dibromide; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane; 1.1: |Grignard Reaction / 1.2: |Grignard Reaction / 2.1: |Wittig Olefination / 2.2: |Wittig Olefination;
DOI:10.3762/bjoc.10.128

Reference yield:

: 1642593-73-4
C₁₅H₂₀O₃

: 1642593-65-4
1-(2,4-dimethoxyphenyl)-4,4-dimethyl-2,3-dioxabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 16 h / 0 - 20 °C / Inert atmosphere

2.1: 2,4,6-tri-(p-methoxyphenyl) pyrylium tetrafluoroborate; oxygen / 1,2-dichloro-ethane / 3 h / -10 °C / 760.05 Torr / Inert atmosphere; UV-irradiation

With potassium tert-butylate; oxygen; 2,4,6-tri-(p-methoxyphenyl) pyrylium tetrafluoroborate; In tetrahydrofuran; 1,2-dichloro-ethane; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.3762/bjoc.10.128