meta-ferrocenyl ethyl benzoate

Base Information

• Chemical Name: meta-ferrocenyl ethyl benzoate
• CAS No.: 12290-30-1
• Molecular Formula: C₁₉H₁₈FeO₂
• Molecular Weight: 334.198
• Mol file: 12290-30-1.mol

Synonyms:meta-ferrocenyl ethyl benzoate

Chemical Property of meta-ferrocenyl ethyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of meta-ferrocenyl ethyl benzoate

There total 1 articles about meta-ferrocenyl ethyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

3-aminobenzoic acid ethyl ester (582-33-2) + ferrocene (102-54-5,55404-68-7) → meta-ferrocenyl ethyl benzoate (12290-30-1)

Guidance literature:

3-aminobenzoic acid ethyl ester; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃; Inert atmosphere; Schlenk technique;

ferrocene; With cetyltrimethylammonium chloride; In diethyl ether; water; at 0 - 20 ℃; for 2h;

DOI:10.1002/cmdc.201700576

Reference yield:

meta-ferrocenyl ethyl benzoate (12290-30-1) → meta-ferrocenyl benzoic acid (12094-13-2)

Guidance literature:

With sodium hydroxide; In methanol; water; Fe-compound treated with 10% NaOH soln.;

DOI:10.1016/j.inoche.2005.01.031

Reference yield:

meta-ferrocenyl ethyl benzoate (12290-30-1) → 3-ferrocenylbenzyl alcohol

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1002/cmdc.201700576

upstream raw materials:

3-aminobenzoic acid ethyl ester

ferrocene

Downstream raw materials:

meta-ferrocenyl benzoic acid