1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate

Base Information

Chemical Name:1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate
CAS No.:68244-25-7
Molecular Formula:C₁₈H₂₃NO₈S
Molecular Weight:413.449
Hs Code.:

Synonyms:1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate

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Chemical Property of 1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate

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Technology Process of 1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate

There total 2 articles about 1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68244-21-3
5-O-carbamoyl-6-chloro-6-deoxy-1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose

: 68244-25-7
1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / sodium metal / tetrahydrofuran / 16 h / Ambient temperature

2: 98 percent / BuLi / tetrahydrofuran; hexane / 1.5 h / Ambient temperature

3: 84 percent / triethylamine / CHCl₃ / 48 h / Ambient temperature

With n-butyllithium; sodium; triethylamine; In tetrahydrofuran; hexane; chloroform;

Reference yield:

: 43138-65-4
1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose

: 68244-25-7
1,2-O-isopropylidene-3-O-methyl-α-D-glucofuranose-5,6-(N-p-tolylsulphonyl)iminocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / BuLi / tetrahydrofuran; hexane / 1.5 h / Ambient temperature

2: 84 percent / triethylamine / CHCl₃ / 48 h / Ambient temperature

With n-butyllithium; triethylamine; In tetrahydrofuran; hexane; chloroform;