(2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

Base Information

Chemical Name:(2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane
CAS No.:1000018-97-2
Molecular Formula:C₃₃H₃₄FNO₈
Molecular Weight:591.633
Hs Code.:

Synonyms:(2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

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Chemical Property of (2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

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Technology Process of (2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

There total 1 articles about (2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1000018-93-8
(2R/S)-3-C-(3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

: 1000018-97-2
(2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at -78 ℃; for 0.75h;
DOI:10.1039/b711531h

Reference yield: 97.0%

: 1000018-97-2
(2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

: 208644-70-6
phenyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1000019-01-1
(2R/S)-3-C-(3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane

Guidance literature:: phenyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; With 1,1'-sulfinylbisbenzene; In dichloromethane;

(2R/S)-3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1-fluoro-2-acetoxypropane; With 4 A molecular sieve; trifluoromethanesulfonic acid anhydride; In dichloromethane; at -60 - 0 ℃; for 5h; Further stages.;
DOI:10.1039/b711531h