C₂₅H₂₂N₆O₃

Base Information

Chemical Name:C₂₅H₂₂N₆O₃
CAS No.:1466565-13-8
Molecular Formula:C₂₅H₂₂N₆O₃
Molecular Weight:454.488
Hs Code.:

C<sub>25</sub>H<sub>22</sub>N<sub>6</sub>O<sub>3</sub>

Synonyms:C₂₅H₂₂N₆O₃

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Chemical Property of C₂₅H₂₂N₆O₃

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Technology Process of C₂₅H₂₂N₆O₃

There total 10 articles about C₂₅H₂₂N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1466564-97-5
(S)-2-amino-N-(1-(8-formyl-1-oxo-2-phenyl-1,2-dihydroisoquinolin-3-yl)ethyl)pyrazolo[1,5-a]pyrimidine-3-carboxamide hydrochloride

: 1466565-13-8
C₂₅H₂₂N₆O₃

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h;

Reference yield:

: 21327-86-6
2-chloro-6-methylbenzoic acid

: 1466565-13-8
C₂₅H₂₂N₆O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 20 °C

1.2: 2 h / 25 - 40 °C / Cooling with ice

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

2.2: 2 h / -30 - -10 °C / Inert atmosphere

2.3: 10.5 h / 20 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: sodium carbonate; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II) / water; 1,4-dioxane / 2 h / 95 °C / Inert atmosphere

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

7.1: sodium periodate / tetrahydrofuran; water / 24 h / 20 °C

8.1: sodium tetrahydroborate / methanol / 1 h / 20 °C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; oxalyl dichloride; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); sodium carbonate; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 1386861-46-6
2-chloro-6-methyl-N-phenylbenzamide

: 1466565-13-8
C₂₅H₂₂N₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

1.2: 2 h / -30 - -10 °C / Inert atmosphere

1.3: 10.5 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.1: sodium carbonate; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II) / water; 1,4-dioxane / 2 h / 95 °C / Inert atmosphere

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

6.1: sodium periodate / tetrahydrofuran; water / 24 h / 20 °C

7.1: sodium tetrahydroborate / methanol / 1 h / 20 °C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); sodium carbonate; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;