1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol

Base Information

• Chemical Name: 1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol
• CAS No.: 253129-15-6
• Molecular Formula: C₂₄H₂₂F₁₂O₂Si
• Molecular Weight: 598.504

Synonyms:1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol

Chemical Property of 1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol

Chemical Property:

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Technology Process of 1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol

There total 2 articles about 1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert.-butyl lithium (594-19-4) + 1-Phenyl-3,3-bis-trifluoromethyl-1-vinyl-1,3-dihydro-benzo[c][1,2]oxasilole (143238-22-6) → 1-((E)-3,3-Dimethyl-but-1-enyl)-1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilole (143238-27-1) + 1-(3,3-Dimethyl-butyl)-1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilole (143238-26-0) + 1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol (253129-15-6)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid; Hexafluoroacetone; Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00045a063

Reference yield:

tert.-butyl lithium (594-19-4) + 1-Phenyl-3,3-bis-trifluoromethyl-1-vinyl-1,3-dihydro-benzo[c][1,2]oxasilole (143238-22-6) + Hexafluoroacetone (684-16-2) → 1-((E)-3,3-Dimethyl-but-1-enyl)-1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilole (143238-27-1) + 1-(3,3-Dimethyl-butyl)-1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilole (143238-26-0) + 1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol (253129-15-6)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid; Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00045a063

Reference yield: 100.0%

1,1,1-Trifluoro-5,5-dimethyl-3-(1-phenyl-3,3-bis-trifluoromethyl-1,3-dihydro-benzo[c][1,2]oxasilol-1-yl)-2-trifluoromethyl-hexan-2-ol (253129-15-6) → C24H21F12O2Si(1-)*Li(1+)

Guidance literature:

With n-butyllithium; In tetrahydrofuran;

DOI:10.1021/ja00045a063

upstream raw materials:

tert.-butyl lithium

1-Phenyl-3,3-bis-trifluoromethyl-1-vinyl-1,3-dihydro-benzo[c][1,2]oxasilole

Hexafluoroacetone

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