(R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

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Chemical Name:(R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid
CAS No.:879502-52-0
Molecular Formula:C₁₉H₂₇NO₇
Molecular Weight:381.426
Hs Code.:

Synonyms:(R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

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Chemical Property of (R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

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Technology Process of (R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

There total 3 articles about (R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 83461-40-9,84806-02-0
methanesulfonic acid (R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 879502-52-0
(R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

Guidance literature:: N-(tert-butoxycarbonyl)-D-(4-hydroxyphenyl)glycine; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.5h;

methanesulfonic acid (R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester; In DMF (N,N-dimethyl-formamide); at 20 - 100 ℃;

Reference yield: 96.0%

: 947183-05-3
2,5-dichloro-benzenesulfonic acid (R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 879502-52-0
(R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

Guidance literature:: N-(tert-butoxycarbonyl)-D-(4-hydroxyphenyl)glycine; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

2,5-dichloro-benzenesulfonic acid (R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester; In N,N-dimethyl-formamide; at 20 - 100 ℃; for 0.25h;

With hydrogenchloride; In water; N,N-dimethyl-formamide; at 0 ℃; pH=4;

Reference yield: 96.0%

: 947183-05-3
2,5-dichloro-benzenesulfonic acid (R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 27460-85-1
N-(tert-butoxycarbonyl)-D-(4-hydroxyphenyl)glycine

: 879502-52-0
(R)-tert-Butoxycarbonylamino-[4-((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetic acid

Guidance literature:: N-(tert-butoxycarbonyl)-D-(4-hydroxyphenyl)glycine; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

2,5-dichloro-benzenesulfonic acid (R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester; In N,N-dimethyl-formamide; at 20 - 100 ℃; for 0.25h;