2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

Base Information

Chemical Name:2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone
CAS No.:943516-03-8
Molecular Formula:C₁₂H₁₂N₂O₄S
Molecular Weight:280.304
Hs Code.:

2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ<sup>2</sup>-5-oxazolinone

Synonyms:2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

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Chemical Property of 2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

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Technology Process of 2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

There total 1 articles about 2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.2%

: 65084-34-6
N-(3-nitrobenzoyl)-methionine

: 943516-03-8
2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

Guidance literature:: With acetic anhydride; at 65 - 70 ℃; for 0.5h;
DOI:10.3390/12010103

Reference yield: 54.78%

: 943516-03-8
2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

: 952155-02-1
N-(3-nitrobenzoyl)-methionyl-hydrazide

Guidance literature:: With hydrazine hydrate; In 1,4-dioxane; water; at 65 - 70 ℃; for 1h;
DOI:10.3390/12010103

Reference yield:

: 943516-03-8
2-(3-nitrophenyl)-4-[2-(methylthio)ethyl]-Δ²-5-oxazolinone

: 952155-09-8
1-[N-(3-nitrobenzoyl)-methionyl]-4-(4-bromophenyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 54.78 percent / hydrazine hydrate / dioxane; H₂O / 1 h / 65 - 70 °C

2: 73.05 percent / methanol / 2 h / 70 - 80 °C

With hydrazine hydrate; In 1,4-dioxane; methanol; water;
DOI:10.3390/12010103