triphenylphosphonium(3-phenylpropadien-1-yl) ylide

Base Information

• Chemical Name: triphenylphosphonium(3-phenylpropadien-1-yl) ylide
• CAS No.: 462113-46-8
• Molecular Formula: C₂₇H₂₁P
• Molecular Weight: 376.438
• Mol file: 462113-46-8.mol

Synonyms:triphenylphosphonium(3-phenylpropadien-1-yl) ylide

Chemical Property of triphenylphosphonium(3-phenylpropadien-1-yl) ylide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of triphenylphosphonium(3-phenylpropadien-1-yl) ylide

There total 1 articles about triphenylphosphonium(3-phenylpropadien-1-yl) ylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

triphenyl(3-phenylprop-1-yn-1-yl)phosphonium bromide → triphenylphosphonium(3-phenylpropadien-1-yl) ylide (462113-46-8)

Guidance literature:

With piperidine; In benzene; for 7h; Heating;

DOI:10.1023/A:1015034402464

Reference yield: 50.0%

triphenylphosphonium(3-phenylpropadien-1-yl) ylide (462113-46-8) → triphenyl(3-phenylprop-1-yn-1-yl)phosphonium bromide

Guidance literature:

With hydrogen bromide; In dichloromethane; for 15h;

DOI:10.1023/A:1015034402464

Reference yield:

triphenylphosphonium(3-phenylpropadien-1-yl) ylide (462113-46-8) → (3-Phenyl-acetonyl)-triphenylphosphoniumbromid (19874-73-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 50 percent / aq. HBr / CH₂Cl₂ / 15 h

2: aq, HBr

With hydrogen bromide; In dichloromethane;

DOI:10.1023/A:1015034402464

Downstream raw materials:

(3-Phenyl-acetonyl)-triphenylphosphoniumbromid