(3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene

Base Information

• Chemical Name: (3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene
• CAS No.: 1000153-31-0
• Molecular Formula: C₂₆H₃₂O₄
• Molecular Weight: 408.538

Synonyms:(3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene

Chemical Property of (3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene

Chemical Property:

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Technology Process of (3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene

There total 1 articles about (3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

(PMBOCH2CH2C)2 + 2,3-butadien-1-ol (18913-31-0) → (3E)-1-(4-methoxybenzyloxy)-4-(2-(4-methoxybenzyloxy)ethyl)-5-vinyl-3,5-hexadiene (1000153-31-0) + (2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)octa-2,5-dien-1-ol (1000153-23-0)

Guidance literature:

(PMBOCH₂CH₂C)2; With triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride; In diethyl ether; hexane; toluene; at -78 - -30 ℃;

2,3-butadien-1-ol; With n-butyllithium; In diethyl ether; hexane; toluene; at -78 - -30 ℃; Further stages.;

DOI:10.1039/b708256h

upstream raw materials:

2,3-butadien-1-ol

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