6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

Base Information

Chemical Name:6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol
CAS No.:1073437-14-5
Molecular Formula:C₁₄H₁₉F₂NO₄
Molecular Weight:303.306
Hs Code.:

Synonyms:6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

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Chemical Property of 6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

Chemical Property:

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Technology Process of 6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

There total 1 articles about 6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1075700-99-0
6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluoro-benzaldehyde

: 1073437-14-5
6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

Guidance literature:: 6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluoro-benzaldehyde; With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; Cooling with ice;

With water; In tetrahydrofuran;

Reference yield:

: 1073437-14-5
6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

: 610-78-6
3-nitro-4-chlorophenol

: C₂₀H₂₁ClF₂N₂O₆

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 84478-87-5
2-bromo-4-fluoro-5-nitro-phenol

: 1073437-14-5
6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol

: 1075700-83-2
6-{6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyloxy}-3-fluoro-4-nitro-1-bromobenzene

Guidance literature:: 6-[2-(tert-butoxycarbonylamino)ethoxy]-2,3-difluorobenzyl alcohol; With methanesulfonyl chloride; triethylamine; In ethyl acetate; Cooling with ice;

With lithium bromide; In ethyl acetate; at 60 ℃; for 0.5h;

2-bromo-4-fluoro-5-nitro-phenol; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;