C₁₃H₁₉BrO

Base Information

• Chemical Name: C₁₃H₁₉BrO
• CAS No.: 1037147-28-6
• Molecular Formula: C₁₃H₁₉BrO
• Molecular Weight: 271.197
• Mol file: 1037147-28-6.mol

Synonyms:C₁₃H₁₉BrO

Chemical Property of C₁₃H₁₉BrO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₉BrO

There total 1 articles about C₁₃H₁₉BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-Bromoheptane (629-04-9) + 2-hydroxybromobenzene (95-56-7) → C13H19BrO (1037147-28-6)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 60 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.joc.6b00733

Reference yield: 91.0%

C13H19BrO (1037147-28-6) → n-phenoxyheptane (32395-96-3)

Guidance literature:

C₁₃H₁₉BrO; With n-butyllithium; 1,1-diethyl-3-ethylurea; In tetrahydrofuran; hexane; at 0 ℃; for 0.0833333h; Inert atmosphere;

With samarium diiodide; tert-Amyl alcohol; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.6b00733

upstream raw materials:

1-Bromoheptane

2-hydroxybromobenzene

Downstream raw materials:

n-phenoxyheptane