C₅₀H₆₂O₅SSi

Base Information

• Chemical Name: C₅₀H₆₂O₅SSi
• CAS No.: 1438276-41-5
• Molecular Formula: C₅₀H₆₂O₅SSi
• Molecular Weight: 803.191
• Mol file: 1438276-41-5.mol

Synonyms:C₅₀H₆₂O₅SSi

Chemical Property of C₅₀H₆₂O₅SSi

Chemical Property:

Purity/Quality:

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Technology Process of C₅₀H₆₂O₅SSi

There total 2 articles about C₅₀H₆₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C29H36O4S (1438275-88-7) + tert-Butyl-(cyclopent-1-enyloxy)-diphenyl-silane (90036-86-5) → C50H62O5SSi (1438276-41-5)

Guidance literature:

With copper(II) perchlorate hexahydrate; C₂₄H₃₆N₂O₅; In dichloromethane; at 30 ℃; stereoselective reaction; Inert atmosphere; Molecular sieve;

DOI:10.1002/anie.201300032

Reference yield:

C28H34O4S (1438276-82-4) → C50H62O5SSi (1438276-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / Inert atmosphere

1.2: Inert atmosphere

2.1: copper(II) perchlorate hexahydrate; C₂₄H₃₆N₂O₅ / dichloromethane / 30 °C / Inert atmosphere; Molecular sieve

With copper(II) perchlorate hexahydrate; C₂₄H₃₆N₂O₅; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; mineral oil;

DOI:10.1002/anie.201300032

upstream raw materials:

C₂₈H₃₄O₄S

C₂₉H₃₆O₄S

tert-Butyl-(cyclopent-1-enyloxy)-diphenyl-silane

Refernces