C₂₇H₃₃N₅O₃Si

Base Information

Chemical Name:C₂₇H₃₃N₅O₃Si
CAS No.:1425044-93-4
Molecular Formula:C₂₇H₃₃N₅O₃Si
Molecular Weight:503.676
Hs Code.:

C<sub>27</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>Si

Synonyms:C₂₇H₃₃N₅O₃Si

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Chemical Property of C₂₇H₃₃N₅O₃Si

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Technology Process of C₂₇H₃₃N₅O₃Si

There total 2 articles about C₂₇H₃₃N₅O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425044-92-3
C₂₇H₃₂N₂O₃Si

: 1425044-93-4
C₂₇H₃₃N₅O₃Si

Guidance literature:: With L-ascorbic acid sodium salt; trimethylsilylazide; copper(II) sulfate; In water; dimethyl sulfoxide; at 80 ℃; for 17h;

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1425044-93-4
C₂₇H₃₃N₅O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: XPhos; dichloro bis(acetonitrile) palladium(II); caesium carbonate / acetonitrile / 2 h / 20 - 95 °C / Inert atmosphere

2: trimethylsilylazide; L-ascorbic acid sodium salt; copper(II) sulfate / water; dimethyl sulfoxide / 17 h / 80 °C

With dichloro bis(acetonitrile) palladium(II); L-ascorbic acid sodium salt; trimethylsilylazide; caesium carbonate; copper(II) sulfate; XPhos; In water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 1393179-35-5
2-amino-4-chloropyrimidine-5-carbonitrile

: 1425044-93-4
C₂₇H₃₃N₅O₃Si

: 1425043-06-6
C₂₄H₁₉N₉O

Guidance literature:: C₂₇H₃₃N₅O₃Si; With trifluoroacetic acid; In dichloromethane; at 22 ℃; for 1h;

2-amino-4-chloropyrimidine-5-carbonitrile; With N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 110 ℃; for 15h;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; for 4.5h; Cooling;