12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.0^2,7>-2,4,6-dodecatriene

Base Information

• Chemical Name: 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.0^2,7>-2,4,6-dodecatriene
• CAS No.: 116911-90-1
• Molecular Formula: C₁₅H₂₀O₂
• Molecular Weight: 232.323

Synonyms:12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.0^2,7>-2,4,6-dodecatriene

Chemical Property of 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.0^2,7>-2,4,6-dodecatriene

Chemical Property:

Purity/Quality:

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Technology Process of 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.0^2,7>-2,4,6-dodecatriene

There total 4 articles about 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.0^2,7>-2,4,6-dodecatriene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5-dimethyl-6-hydroxy-6-(3',5'-dimethoxy-4'-hydroxyphenyl)-1-hexene (116911-85-4) → syringic alcohol (530-56-3) + 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-90-1) + 12,12-dimethyl-5-hydroxy-4-methoxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-89-8) + 12,12-dimethyl-4,6-dimethoxy-5-hydroxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-88-7)

Guidance literature:

With sodium hydroxide; at 135 ℃; for 18h; Further byproducts given;

DOI:10.1021/jo00258a006

Reference yield:

5,5-dimethyl-6-hydroxy-6-(3',5'-dimethoxy-4'-hydroxyphenyl)-1-hexene (116911-85-4) → syringic alcohol (530-56-3) + 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-90-1) + 12,12-dimethyl-5-hydroxy-4-methoxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-89-8) + trans-2-(3',5'-dimethoxy-4'-hydroxyphenyl)-1,1,3-trimethylcyclopentane (116911-87-6)

Guidance literature:

With sodium hydroxide; D-glucose; at 135 ℃; for 18h; Further byproducts given;

DOI:10.1021/jo00258a006

Reference yield:

5,5-dimethyl-6-hydroxy-6-(3',5'-dimethoxy-4'-hydroxyphenyl)-1-hexene (116911-85-4) → syringic alcohol (530-56-3) + 12,12-dimethyl-5-hydroxy-6-methoxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-90-1) + 12,12-dimethyl-5-hydroxy-4-methoxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-89-8) + 12,12-dimethyl-4,6-dimethoxy-5-hydroxytricyclo<7.3.0.02,7>-2,4,6-dodecatriene (116911-88-7) + trans-2-(3',5'-dimethoxy-4'-hydroxyphenyl)-1,1,3-trimethylcyclopentane (116911-87-6) + cis-2-(3',5'-dimethoxy-4'-hydroxyphenyl)-1,1,3-trimethylcyclopentane (116911-87-6)

Guidance literature:

With sodium hydroxide; D-glucose; at 135 ℃; Product distribution; Mechanism; other (or without) additive; other reaction time;

DOI:10.1021/jo00258a006

upstream raw materials:

5,5-dimethyl-6-hydroxy-6-(3',5'-dimethoxy-4'-hydroxyphenyl)-1-hexene

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