1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

Base Information

Chemical Name:1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]
CAS No.:1026919-61-8
Molecular Formula:C₂₅H₁₈ClN₅O₂
Molecular Weight:455.903
Hs Code.:

1-(4-chloro-phenyl)-1<i>H</i>-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

Synonyms:1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

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Chemical Property of 1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

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Technology Process of 1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

There total 6 articles about 1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-09-8
ethyl 3-(2-furyl)-3-oxopropanoate

: 1026919-61-8
1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

Guidance literature:: Multi-step reaction with 6 steps

1: TsOH / ethanol / 3 h / Heating

2: NaIO₄; RuCl₃ / acetonitrile; H₂O; CCl₄

3: POCl₃; pyridine

4: NaOH / H₂O; methanol

5: (COCl)2 / DMF / CH₂Cl₂

6: pyridine / CH₂Cl₂

With pyridine; ruthenium trichloride; sodium hydroxide; sodium periodate; oxalyl dichloride; toluene-4-sulfonic acid; trichlorophosphate; N,N-dimethyl-formamide; In methanol; tetrachloromethane; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm020112w

Reference yield:

: 1-(4-chloro-phenyl)-5-(4-cyano-phenylcarbamoyl)-1H-pyrazole-3-carboxylic acid

: 1026919-61-8
1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2 / DMF / CH₂Cl₂

2: pyridine / CH₂Cl₂

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jm020112w

Reference yield:

: 1026798-82-2
1-(4-chloro-phenyl)-5-(4-cyano-phenylcarbamoyl)-1H-pyrazole-3-carboxylic acid ethyl ester

: 1026919-61-8
1-(4-chloro-phenyl)-1H-pyrazole-3,5-dicarboxylic acid 3-benzylamide 5-[(4-cyano-phenyl)-amide]

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / H₂O; methanol

2: (COCl)2 / DMF / CH₂Cl₂

3: pyridine / CH₂Cl₂

With pyridine; sodium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In methanol; dichloromethane; water;
DOI:10.1021/jm020112w