2-(2-Oxopyrrolidin-1-yl)ethyl 2-methylprop-2-enoate

Base Information

• Chemical Name: 2-(2-Oxopyrrolidin-1-yl)ethyl 2-methylprop-2-enoate
• CAS No.: 946-25-8
• Molecular Formula: C₁₀H₁₅NO₃
• Molecular Weight: 197.234
• Hs Code.: 2933790090
• DSSTox Substance ID: DTXSID10431548
• Nikkaji Number: J364.806K
• Wikidata: Q82245458
• Mol file: 946-25-8.mol

Synonyms:946-25-8;METHACRYLIC ACID 2-(2-OXO-1-PYRROLIDINYL)ETHYL ESTER;2-(2-oxopyrrolidin-1-yl)ethyl 2-methylprop-2-enoate;2-(2-oxopyrrolidin-1-yl)ethyl methacrylate;SCHEMBL163326;DTXSID10431548;XVTPGZQPUZSUKS-UHFFFAOYSA-N;N-(2-methacryloyloxyethyl)pyrrolidone;1-(2-methacryloyloxyethyl)-2-pyrrolidone;AS-77345;D94302;Methacrylic acid 2-(2-oxopyrrolizino)ethyl ester;2-Propenoic acid, 2-methyl-, 2-(2-oxo-1-pyrrolidinyl)ethyl ester

Chemical Property of 2-(2-Oxopyrrolidin-1-yl)ethyl 2-methylprop-2-enoate

Chemical Property:

• PSA: 46.61000
• LogP: 0.66600
• XLogP3: 0.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 197.10519334
• Heavy Atom Count: 14
• Complexity: 260

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C(=O)OCCN1CCCC1=O

Technology Process of 2-(2-Oxopyrrolidin-1-yl)ethyl 2-methylprop-2-enoate

There total 3 articles about 2-(2-Oxopyrrolidin-1-yl)ethyl 2-methylprop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-(2-hydroxyethyl)-2-pyrrolidinone (3445-11-2) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → N-(2-methacryloyloxyethyl)pyrrolidone (946-25-8)

Guidance literature:

With 10H-phenothiazine; 4-methoxy-phenol; sodium methylate; at 60 - 88 ℃; for 5h; Product distribution / selectivity;

Reference yield: 24.0%

1-(2-hydroxyethyl)-2-pyrrolidinone (3445-11-2) + Methacryloyl chloride (920-46-7,26937-45-1) → N-(2-methacryloyloxyethyl)pyrrolidone (946-25-8)

Guidance literature:

With triethylamine; In chloroform; at 5 - 10 ℃; for 11h; Inert atmosphere;

DOI:10.1002/pola.27208

Reference yield:

→ N-(2-methacryloyloxyethyl)pyrrolidone (946-25-8)

Guidance literature:

N-(2-Hydroxy-ethyl)-pyrrolidinon, Methacrylsaeure-methylester/Natriummethylat <4-Hydroxy-diphenylamin>;

upstream raw materials:

1-(2-hydroxyethyl)-2-pyrrolidinone

methacrylic acid methyl ester

Methacryloyl chloride

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