10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

Base Information

Chemical Name:10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene
CAS No.:110036-23-2
Molecular Formula:C₂₄H₂₂O₂
Molecular Weight:342.437
Hs Code.:

Synonyms:10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

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Chemical Property of 10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

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Technology Process of 10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

There total 6 articles about 10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 13732-58-6
(E)-4,4'-(1-phenylbut-1-ene-1,2-diyl)bis(methoxybenzene)

: 110036-23-2
10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

: 10-Ethyl-3,6-dimethoxy-9-phenylphenanthrene

Guidance literature:: With iodine; In cyclohexane; for 3h; Irradiation;
DOI:10.1002/ardp.19873200212

Reference yield:

: 500309-64-8
4-methoxy-2-phenyl-benzyl alcohol

: 110036-23-2
10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

Guidance literature:: Multi-step reaction with 5 steps

1: PBr₃; diethyl ether / anschliessend mit KCN in wss. Aethanol behandeln

2: NaNH₂

3: diethyl ether / beim Erwaermen des Reaktionsgemisches mit wss. HCl

4: aqueous HBr; acetic acid

With diethyl ether; hydrogen bromide; phosphorus tribromide; sodium amide; acetic acid;
DOI:10.1021/ja01139a043

Reference yield:

: 861069-43-4
(5-methoxy-biphenyl-2-yl)-acetonitrile

: 110036-23-2
10-Ethyl-3-methoxy-9-(4-methoxyphenyl)-phenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: NaNH₂

2: diethyl ether / beim Erwaermen des Reaktionsgemisches mit wss. HCl

3: aqueous HBr; acetic acid

With diethyl ether; hydrogen bromide; sodium amide; acetic acid;
DOI:10.1021/ja01139a043