1,6-dibromo-2-methoxy-3-benzylnaphthalene

Base Information

Chemical Name:1,6-dibromo-2-methoxy-3-benzylnaphthalene
CAS No.:1346998-31-9
Molecular Formula:C₁₈H₁₄Br₂O
Molecular Weight:406.117
Hs Code.:

Synonyms:1,6-dibromo-2-methoxy-3-benzylnaphthalene

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Chemical Property of 1,6-dibromo-2-methoxy-3-benzylnaphthalene

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Technology Process of 1,6-dibromo-2-methoxy-3-benzylnaphthalene

There total 11 articles about 1,6-dibromo-2-methoxy-3-benzylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: C₁₈H₁₄Br₂O₂

: 1346998-31-9
1,6-dibromo-2-methoxy-3-benzylnaphthalene

: 1346998-33-1
3-benzyl-1,6-dibromonaphthalen-2-ol

Guidance literature:: C₁₈H₁₄Br₂O₂; With sodium tetrahydroborate; In tetrahydrofuran; for 0.5h; Cooling with ice;

With aluminum (III) chloride; In tetrahydrofuran; at 20 ℃; for 20h; Reflux;
DOI:10.1016/j.bioorg.2020.104054

Reference yield:

: 1779-10-8
1,6-dibromo-2-hydroxynaphthalene-3-carboxylic acid

: 1346998-31-9
1,6-dibromo-2-methoxy-3-benzylnaphthalene

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 10 h / Reflux

2.1: lithium aluminium tetrahydride / diethyl ether / 5 h / Inert atmosphere; Reflux

3.1: manganese(IV) oxide / acetone / 48 h / 20 °C

4.1: iodine; magnesium / tetrahydrofuran / 3 h / Reflux

4.2: 1.5 h / Reflux

5.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / Cooling with ice

5.2: 20 h / 20 °C / Reflux

With manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; iodine; potassium carbonate; magnesium; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/j.bioorg.2020.104054

Reference yield:

: 175204-91-8
methyl 4,7-dibromo-3-methoxynaphthalene-2-carboxylate

: 1346998-31-9
1,6-dibromo-2-methoxy-3-benzylnaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 5 h / Inert atmosphere; Reflux

2.1: manganese(IV) oxide / acetone / 48 h / 20 °C

3.1: iodine; magnesium / tetrahydrofuran / 3 h / Reflux

3.2: 1.5 h / Reflux

4.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / Cooling with ice

4.2: 20 h / 20 °C / Reflux

With manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; iodine; magnesium; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/j.bioorg.2020.104054