2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

Base Information

Chemical Name:2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside
CAS No.:338796-43-3
Molecular Formula:C₂₀H₃₁NO₁₀S
Molecular Weight:477.533
Hs Code.:

Synonyms:2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

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Chemical Property of 2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

Chemical Property:

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Technology Process of 2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

There total 4 articles about 2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 98-59-9
p-toluenesulfonyl chloride

: 338796-42-2
2-tert-butyloxycarbonylamidoethyl α-D-mannopyranoside

: 338796-43-3
2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1021/jo005671u

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 338796-43-3
2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / Pd-C / ethyl acetate / 6 h / 20 °C

2: 94 percent / NH₃ / methanol / 2 h / 0 °C

3: 68 percent / Py / 0 - 20 °C

With pyridine; ammonia; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jo005671u

Reference yield:

: 140428-83-7
2-azidoethyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 338796-43-3
2-tert-butyloxycarbonylamidoethyl 6-O-(toluene-4-sulfonyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / Pd-C / ethyl acetate / 6 h / 20 °C

2: 94 percent / NH₃ / methanol / 2 h / 0 °C

3: 68 percent / Py / 0 - 20 °C

With pyridine; ammonia; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jo005671u