6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

Base Information

Chemical Name:6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl
CAS No.:455317-91-6
Molecular Formula:C₃₆H₄₀Cl₂N₄O₂
Molecular Weight:631.645
Hs Code.:

Synonyms:6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

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Chemical Property of 6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

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Technology Process of 6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

There total 3 articles about 6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 455317-78-9
6,6'-bis{1-[N-((1S)-2-hydroxy-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

: 455317-91-6
6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

Guidance literature:: With thionyl chloride; In chloroform; at 20 ℃;
DOI:10.1016/S0957-4166(02)00069-1

Reference yield:

: 49669-22-9
6,6'-Dibromo-2,2'-bipyridine

: 455317-91-6
6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran; hexane / 0.67 h / -78 °C

1.2: 98 percent / tetrahydrofuran; hexane / 0.17 h / -78 °C / Irradiation

2.1: 78 percent / NaCN / xylene / 168 h / Heating

3.1: 90 percent / SOCl₂ / CHCl₃ / 20 °C

With thionyl chloride; sodium cyanide; lithium diisopropyl amide; In tetrahydrofuran; hexane; chloroform; xylene;
DOI:10.1016/S0957-4166(02)00069-1

Reference yield:

: 455317-76-7
6,6'-bis(1-ethoxycarbonyl-1-methylethyl)-[2,2']bipyridinyl

: 455317-91-6
6,6'-bis{1-[N-((1S)-2-chloro-1-benzyl-ethyl)]carbamoyl-1-methyl-ethyl}-[2,2']bipyridinyl

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaCN / xylene / 168 h / Heating

2: 90 percent / SOCl₂ / CHCl₃ / 20 °C

With thionyl chloride; sodium cyanide; In chloroform; xylene;
DOI:10.1016/S0957-4166(02)00069-1