<(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester

Base Information

• Chemical Name: <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester
• CAS No.: 73183-83-2
• Molecular Formula: C₂₉H₃₀N₂O₆
• Molecular Weight: 502.567

Synonyms:<(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester

Chemical Property of <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester

Chemical Property:

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Technology Process of <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester

There total 3 articles about <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

o-iodo-methyl-benzoic acid (610-97-9) + 2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-amin (73183-82-1) → <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester (73183-83-2)

Guidance literature:

With potassium carbonate; Naturkupfer C;

Reference yield:

1,1,3,3-tetramethyl-5-hydroxy indane (53718-26-6) → <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester (73183-83-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 47 percent / NaNO₂, conc. HNO₃ / acetic acid / 0.25 h / 10 - 20 °C

2: 88 percent / sat. aq. NH₃, NH₄Cl / 20 h / 140 - 150 °C / 18751.5 Torr

3: 24 percent / K₂CO₃ / Naturkupfer C

With ammonium hydroxide; nitric acid; potassium carbonate; ammonium chloride; sodium nitrite; Naturkupfer C; In acetic acid;

Reference yield:

2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-ol (73183-80-9) → <(2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester (73183-83-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / sat. aq. NH₃, NH₄Cl / 20 h / 140 - 150 °C / 18751.5 Torr

2: 24 percent / K₂CO₃ / Naturkupfer C

With ammonium hydroxide; potassium carbonate; ammonium chloride; Naturkupfer C;

upstream raw materials:

o-iodo-methyl-benzoic acid

2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-amin

1,1,3,3-tetramethyl-5-hydroxy indane

2,3-Dihydro-1,1,3,3-tetramethyl-6-nitro-1H-inden-5-ol

Downstream raw materials:

2-<2,3,5,10-Tetrahydro-1,1,3,3-tetramethyl-10-oxo-1H-cyclopentacridin-5-yl>benzoesaeure-methylester

<(2,3-Dihydro-1,1,3,3-tetramethyl-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester

<(2,3-Dihydro-1,1,3,3-tetramethyl-6-amino-1H-inden-5-yl)imino>-2,2'-dibenzoesaeure-dimethylester

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