Technology Process of C26H24N4O8S2
There total 9 articles about C26H24N4O8S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 25 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Oxone / water; isopropyl alcohol / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 42 h / 80 - 120 °C
3: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 18 h / 25 °C
4: potassium carbonate / N,N-dimethyl-formamide / 120 h / 120 °C
5: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 25 °C
With
Oxone; hydrogen; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon;
In
ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / 18 h / 70 °C / Sealed tube; Heating / reflux
2: caesium carbonate / acetone / 18 h / 55 °C / Heating / reflux
3: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 25 °C
With
(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; N-ethyl-N,N-diisopropylamine;
sulfuric acid;
In
dichloromethane; acetone;