22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene

Base Information

Chemical Name:22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene
CAS No.:118356-73-3
Molecular Formula:C₁₇H₂₆O₇
Molecular Weight:342.389
Hs Code.:

22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1<sup>(21)</sup>,18<sup>(22)</sup>,19-triene

Synonyms:22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene

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Technology Process of 22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene

There total 1 articles about 22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118356-72-2
1,3-bis(2-hydroxyethoxy)-2-methoxybenzene

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 118356-73-3
22-Methoxy-2,5,8,11,14,17-hexaoxa-bicyclo[16.3.1]docosa-1⁽²¹⁾,18⁽²²⁾,19-triene

: 118356-82-4
43,44-Dimethoxy-2,5,8,11,14,17,23,26,29,32,35,38-dodecaoxa-tricyclo[37.3.1.1^18,22]tetratetraconta-1⁽⁴³⁾,18,20,22⁽⁴⁴⁾,39,41-hexaene

Guidance literature:: With potassium tert-butylate; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, RT, 1 h, 2a.) RT, overnight, b.) reflux, 72 h;
DOI:10.1021/jo00265a027