methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

Base Information

Chemical Name:methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside
CAS No.:101696-47-3
Molecular Formula:C₂₁H₂₈O₇
Molecular Weight:392.449
Hs Code.:

Synonyms:methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

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Chemical Property of methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

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Technology Process of methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

There total 4 articles about methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 101696-46-2
(R)-2-((3aR,4R,6R,6aR)-6-Methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-3,4-dihydro-2H-pyran-4-ol

: 101696-47-3
methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; paraffin; at 0 ℃;
DOI:10.1021/ja00230a024

Reference yield:

: 33985-40-9
(3aR,4S,6R,6aR)-tetrahydro-6-methoxy-2,2-dimethylfuro-[3,4-d][1,3]dioxole-4-carbaldehyde

: 101696-47-3
methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent

2: NaBH₄-CeCl₃ / methanol

3: NaH

With sodium tetrahydroborate; cerium(III) chloride; sodium hydride; In methanol;
DOI:10.1021/ja00269a080

Reference yield:

: 99441-05-1
methyl 5,9-anhydro-6,8-dideoxy-2,3-O-(1-methylethylidene)-β-D-allo-non-8-enofuranosid-7-ulose

: 101696-47-3
methyl 5,9-anhydro-6,8-dideoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-non-8-enofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄-CeCl₃ / methanol

2: NaH

With sodium tetrahydroborate; cerium(III) chloride; sodium hydride; In methanol;
DOI:10.1021/ja00269a080