1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose

Base Information

• Chemical Name: 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose
• CAS No.: 96689-89-3
• Molecular Formula: C₃₅H₃₈O₇
• Molecular Weight: 570.683

Synonyms:1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose

Chemical Property of 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose

Chemical Property:

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Technology Process of 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose

There total 5 articles about 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,3,5-tri-O-benzyl-D-ribofuranose (16838-89-4) + 1,2,3-trimethoxybenzene (621-23-8) → 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose (96689-89-3)

Guidance literature:

With calcium sulfate; Hexamethyldisiloxane; lanthanum(lll) triflate; In nitromethane; for 3h; Ambient temperature;

DOI:10.1055/s-1994-25695

Reference yield: 65.0%

1,2,3-trimethoxybenzene (621-23-8) + (2R,3R,4R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-(4-methoxy-phenyltellanyl)-tetrahydro-furan → 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose (96689-89-3)

Guidance literature:

With boron trifluoride diethyl etherate; In chloroform; at -10 ℃; for 1h;

Reference yield: 49.0%

1,2,3-trimethoxybenzene (621-23-8) + 2-pyridyl 2,3,5-tri-O-benzyl-D-ribofuranosyl sulfide → 1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-2,3,5-tri-O-benzyl-D-ribofuranose (96689-89-3)

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1021/ja00300a036

upstream raw materials:

1,2,3-trimethoxybenzene

2,3,5-tri-O-benzyl-D-ribofuranose

Methanesulfonic acid (3R,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl ester

Downstream raw materials:

β-1-deoxy-1-(C-2',4',6'-trimethoxyphenyl)-D-ribofuranose

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