3--N-benzylamino>propionitrile

Base Information

Chemical Name:3--N-benzylamino>propionitrile
CAS No.:104283-60-5
Molecular Formula:C₁₄H₁₇N₅
Molecular Weight:255.322
Hs Code.:

3-<N-<(E)-4-azido-2-buten-1-yl>-N-benzylamino>propionitrile

Synonyms:3--N-benzylamino>propionitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--N-benzylamino>propionitrile

Chemical Property:

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Technology Process of 3--N-benzylamino>propionitrile

There total 2 articles about 3--N-benzylamino>propionitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 706-03-6
3-(benzylamino)propionitrile

: 85669-62-1
(Z)-4-acetoxy-2-buten-1-yl diethyl phosphate

: 104283-60-5
3--N-benzylamino>propionitrile

Guidance literature:: With sodium azide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; for 3h;
DOI:10.1016/S0040-4039(00)83983-0

Reference yield:

: 706-03-6
3-(benzylamino)propionitrile

: 104283-60-5
3--N-benzylamino>propionitrile

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(PPh₃)4 / tetrahydrofuran / 2 h / Ambient temperature

2: Pd(PPh₃)4, sodium azide (90percent) / tetrahydrofuran; H₂O / Ambient temperature

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; In tetrahydrofuran; water;
DOI:10.1021/jo00275a011

Reference yield:

: 104283-60-5
3--N-benzylamino>propionitrile

: 120990-21-8
3--N-benzylamino>propionitrile

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; H₂O / 2 h / 50 °C

2: 2 N aq. NaOH / tetrahydrofuran / 1 h / 50 °C

With sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1021/jo00275a011