(1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Base Information

Chemical Name:(1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine
CAS No.:106137-02-4
Molecular Formula:C₁₆H₂₃NO₃
Molecular Weight:277.364
Hs Code.:

Synonyms:(1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Suppliers and Price of (1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

There total 5 articles about (1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 106062-28-6
(3aR,4R,5S,6S,6aS)-4-Azido-6-benzyloxymethyl-5-iodo-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole

: 106137-02-4
(1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 0.75h; Heating;

Reference yield:

: 144069-04-5
5β-benzyloxymethyl-1α,2α,4α-trihydroxy-3β-azidocyclopentane

: 106137-02-4
(1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / p-TsOH / 2 h

2: pyridine / CH₂Cl₂ / 0.5 h / 0 °C

3: LiI / dimethylformamide / 1 h

4: 79 percent / Bu₃SnH, AIBN / benzene / 0.75 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; toluene-4-sulfonic acid; lithium iodide; In dichloromethane; N,N-dimethyl-formamide; benzene;

Reference yield:

: 143994-98-3
(1R,2S,3R,4R,5S)-2-Azido-4-benzyloxymethyl-5-(2-methoxy-ethoxymethoxy)-cyclopentane-1,3-diol

: 106137-02-4
(1S),(1β,2α,3α,4β)-Benzyloxymethyl-2,3-dimethylmethylenedioxycyclopentamine

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / Me₂BBr / CH₂Cl₂; diethyl ether / 2 h / -78 °C

2: 95 percent / p-TsOH / 2 h

3: pyridine / CH₂Cl₂ / 0.5 h / 0 °C

4: LiI / dimethylformamide / 1 h

5: 79 percent / Bu₃SnH, AIBN / benzene / 0.75 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); dimethylboron bromide; tri-n-butyl-tin hydride; toluene-4-sulfonic acid; lithium iodide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene;