(η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2

Base Information

• Chemical Name: (η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2
• CAS No.: 301536-93-6
• Molecular Formula: C₃₂H₄₃FeO₃PSi₂
• Molecular Weight: 618.683

Synonyms:(η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2

Chemical Property of (η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2

Chemical Property:

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Technology Process of (η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2

There total 1 articles about (η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(η5-C5Me5)(CO)2FeP(SiMe3)2 + diphenyl ketene (525-06-4) → (η(5)-Me5C5Fe(CO)2)P(SiMe3)C(OSiMe3)CPh2 (301536-93-6)

Guidance literature:

In pentane; under N2, equimolar amt. of diphenylketene in n-pentane was dropped to n-pentane-soln. of Fe-complex at 0 °C, soln. was warmed up to room temp., stirred for 4 h at this temp.; soln. was evapd. to dryness in vac., residue was taken out in n-pentane, soln. was filtered, concd., crystn. at 0 °C for 3 d, elem. anal.;

DOI:10.1002/1521-3749(200008)626:8<1831::AID-ZAAC1831>3.0.CO;2-5

upstream raw materials:

diphenyl ketene

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