N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester
CAS No.:78221-58-6
Molecular Formula:C₂₇H₂₆Cl₃NO₄S
Molecular Weight:566.933
Hs Code.:

Synonyms:N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

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Chemical Property of N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

There total 3 articles about N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 78221-56-4
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine

: 95-95-4
2,4,5-trichlorophenol

: 78221-58-6
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; 1) 0 deg C, 1 h; 2) room temp., 15 h;
DOI:10.1135/cccc19810286

Reference yield:

: 78221-55-3
S-(2,4,6-trimethylbenzyl)-L-cysteine

: 78221-58-6
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / NaOH / H₂O / 0.5 h / Ambient temperature

2: 92 percent / dicyclohexylcarbodiimide / ethyl acetate / 1) 0 deg C, 1 h; 2) room temp., 15 h

With sodium hydroxide; dicyclohexyl-carbodiimide; In water; ethyl acetate;
DOI:10.1135/cccc19810286

Reference yield:

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 78221-58-6
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine 2,4,5-trichlorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Na, liquid NH₃ / 1) 15 min; 2) 2 h

2: 69 percent / NaOH / H₂O / 0.5 h / Ambient temperature

3: 92 percent / dicyclohexylcarbodiimide / ethyl acetate / 1) 0 deg C, 1 h; 2) room temp., 15 h

With sodium hydroxide; ammonia; sodium; dicyclohexyl-carbodiimide; In water; ethyl acetate;
DOI:10.1135/cccc19810286