4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

Base Information

Chemical Name:4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal
CAS No.:82236-09-7
Molecular Formula:C₁₇H₂₀FN₂O₂*Cl
Molecular Weight:338.809
Hs Code.:

Synonyms:4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

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Chemical Property of 4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

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Technology Process of 4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

There total 1 articles about 4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.9%

: 504-24-5
4-aminopyridine

: 3308-94-9
4-chloro-1-(4-fluorophenyl)-1,1-(ethylenedioxy)butane

: 82236-09-7
4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

Guidance literature:: In xylene; for 4h; Heating;
DOI:10.1248/cpb.30.719

Reference yield: 91.5%

: 82236-09-7
4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

: 82236-10-0
4-amino-1-<3-(4-fluorobenzoyl)propyl>piperidine ethylene acetal

Guidance literature:: With hydrogen; nickel; In ethanol; at 100 ℃; for 19h;
DOI:10.1248/cpb.30.719

Reference yield:

: 82236-09-7
4-amino-1-<3-(4-fluorobenzoyl)propyl>pyridinium chloride ethylene acetal

: 1-<3-(4-fluorobenzoyl)propyl>-4-(2-nitroanilino)piperidine ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 91.5 percent / H₂ / Raney Ni / ethanol / 19 h / 100 °C

2: 61.8 percent / Na₂CO₃ / butan-1-ol / 31 h / Heating

With hydrogen; sodium carbonate; nickel; In ethanol; butan-1-ol;
DOI:10.1248/cpb.30.719