3-bromophenyl dimethylcarbamate

Base Information

Chemical Name:3-bromophenyl dimethylcarbamate
CAS No.:7305-05-7
Molecular Formula:C₉H₁₀BrNO₂
Molecular Weight:244.088
Hs Code.:

Synonyms:3-bromophenyl dimethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromophenyl dimethylcarbamate

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Technology Process of 3-bromophenyl dimethylcarbamate

There total 1 articles about 3-bromophenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 591-20-8
3-Bromophenol

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 7305-05-7
3-bromophenyl dimethylcarbamate

Guidance literature:: 3-Bromophenol; With pyridine; potassium carbonate; In acetonitrile; for 0.333333h;

N,N-Dimethylcarbamoyl chloride; In acetonitrile; for 2h;

Reference yield: 74.0%

: 7305-05-7
3-bromophenyl dimethylcarbamate

: 5-bromo-2-iodophenyl dimethylcarbamate

Guidance literature:: With trifluorormethanesulfonic acid; palladium diacetate; 1-methoxy-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In 1,2-dichloro-ethane; at 20 ℃; for 6h; regioselective reaction; Sealed tube;
DOI:10.1039/c5cc02533h

Reference yield: 73.0%

: 7305-05-7
3-bromophenyl dimethylcarbamate

: 1631050-43-5
5-bromo-2-hydroxyphenyl dimethylcarbamate

Guidance literature:: With dipotassium peroxodisulfate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; trifluoroacetic acid; trifluoroacetic anhydride; at 80 ℃; for 2.5h; regioselective reaction; Sealed tube;
DOI:10.1002/adsc.201300999