(S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole

Base Information

• Chemical Name: (S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole
• CAS No.: 952487-71-7
• Molecular Formula: C₂₀H₂₄N₄O₄S
• Molecular Weight: 416.501

Synonyms:(S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole

Chemical Property of (S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole

Chemical Property:

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Technology Process of (S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole

There total 1 articles about (S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H24N4O2S → (S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole (952487-71-7)

Guidance literature:

With ammonium molybdate(VI) tetrahydrate; dihydrogen peroxide; In ethanol; at 0 - 20 ℃; for 16h;

DOI:10.1016/j.bmcl.2007.06.094

Reference yield: 37.0%

(S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole (952487-71-7) + (2S,3S)-3-<(tertbutyl)dimethylsilyloxy>-2-methylpentanal (108815-17-4) → C25H44O3Si

Guidance literature:

(S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole; With potassium hexamethylsilazane; In 1,2-dimethoxyethane; at -78 ℃; for 0.333333h;

(2S,3S)-3-<(tertbutyl)dimethylsilyloxy>-2-methylpentanal; In 1,2-dimethoxyethane; at -78 - 20 ℃; for 1h; Further stages.;

DOI:10.1016/j.bmcl.2007.06.094

Reference yield:

(S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole (952487-71-7) + (2S,3R)-3-(tert-butyldimethylsilyloxy)-2-methylpentanal (114181-55-4) → C25H44O3Si

Guidance literature:

(S)-5-[4-(benzyloxymethoxy)-3-methylbutylsulfonyl]-1-phenyl-1H-tetrazole; With potassium hexamethylsilazane; In 1,2-dimethoxyethane; at -78 ℃; for 0.333333h;

(2S,3R)-3-(tert-butyldimethylsilyloxy)-2-methylpentanal; In 1,2-dimethoxyethane; at -78 - 20 ℃; for 1h; Further stages.;

DOI:10.1016/j.bmcl.2007.06.094

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