β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1)

Base Information

• Chemical Name: β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1)
• CAS No.: 1197190-86-5
• Molecular Formula: C₉₀H₃₀F₃₀N₆
• Molecular Weight: 1765.22

Synonyms:β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1)

Chemical Property of β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1)

Chemical Property:

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Technology Process of β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1)

There total 1 articles about β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C90H32F30N6 → β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1) (1197190-86-5)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; for 3h;

DOI:10.1039/b910167e

Reference yield: 100.0%

β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1) (1197190-86-5) → C90H32F30N6

Guidance literature:

With sodium tetrahydroborate;

DOI:10.1039/b910167e

Reference yield: 17.0%

β-tetraphenyl meso-hexakis(pentafluorophenyl)[26]hexaphyrin(1.1.1.1.1.1) (1197190-86-5) + palladium dichloride → (C4H2NHCC6F5C4N(C6H5)2CC6F5C4NH2CC6F5)2Pd*2C6H5Cl + (C4H2NHCC6F5C4N(C6H5)2CC6F5C4NH2CC6F5)2Pd*C6H14*CH2Cl2

Guidance literature:

With CH₃COONa; In methanol; dichloromethane; to a soln. of hexaphyrin in CH2Cl2-CH3OH PdCl2 and NaOCOCH3 were added, refluxed for 3 h; the mixt. was poured into water, extd. with CH2Cl2, the organic phase was washed with water, dried over Na2SO4, the solvent was rotary evapd., column silica gel chromy. (10% CH2Cl2/hexane, CH2Cl2), recrystd. from CH2Cl2/hexane;

DOI:10.1246/bcsj.20100053

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