Technology Process of C22H21F5O6S2
There total 5 articles about C22H21F5O6S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H25F5O7S2;
With
tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran;
for 3h;
Heating / reflux;
sodium methansulfinate;
In
tetrahydrofuran;
for 18h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane
2: boron trifluoride diethyl etherate / dichloromethane
3: triethylamine / dichloromethane
4: potassium tert-butylate / tetrahydrofuran
5: ozone / dichloromethane
6: triethylamine
7: tetra-(n-butyl)ammonium iodide / tetrahydrofuran
With
boron trifluoride diethyl etherate; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / tetrahydrofuran
2: ozone / dichloromethane
3: triethylamine
4: tetra-(n-butyl)ammonium iodide / tetrahydrofuran
With
potassium tert-butylate; tetra-(n-butyl)ammonium iodide; ozone; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047